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[1]魏宇,袁军*,冯锦峰,等.N苯基马来酰亚胺的制备与表征[J].武汉工程大学学报,2011,(11):55-58.
　WEI Yu,YUAN Jun,FENG Jin feng,et al.Preparation characterization of Nphenyl maleimide[J].Journal of Wuhan Institute of Technology,2011,(11):55-58.
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N苯基马来酰亚胺的制备与表征(/HTML)
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《武汉工程大学学报》[ISSN:1674-2869/CN:42-1779/TQ]

卷:
期数:
2011年11期
页码:
55-58
栏目:
材料科学与工程
出版日期:
2011-11-30

文章信息/Info

Title:
Preparation characterization of Nphenyl maleimide
文章编号:
16742869(2011)11005504
作者:
魏宇; 袁军*; 冯锦峰; 陈小霞
武汉工程大学材料科学与工程学院，湖北 武汉 430074
Author(s):
WEI Yu; YUAN Jun; FENG Jinfeng; CHEN Xiaoxia
School of Materials Science and Engineering,Wuhan Institute of Technology,Wuhan 430074,China
关键词:
N苯基马来酰亚胺; 顺酐; 离子液体; 合成
Keywords:
Nphenyl maleimide; maleic anhydride; ionic liquids; reaction
分类号:
TQ072
DOI:
-
文献标志码:
AAdoi:10.3969/j.issn.16742869.2011.11.014
摘要:
为了提高N苯基马来酰亚胺的产率与纯度，以顺丁烯二酸酐和苯胺为原料，酸性离子液体作催化剂及脱水剂，对苯二酚为阻聚剂采用两步法制得N苯基马来酰亚胺.结果表明催化剂与原料最佳配比(物质的量的比)为0.0931，产品产率可达86.03%，纯度为97.42%.
Abstract:
To improve the yield and the purity of Nphenyl maleimide,Nphenyl maleimide was produced by the way of twostep method. In this experiment,we used the maleic anhydride and aniline as raw materials,the acidic ionic liquid as catalyst and dehydrating agent,the hydroquinone as inhibitor.The results show that the optimum reaction conditions are as follows:the molar ratio of catalyst and raw materials is 0.0931,the yield of Nphenyl maleimide reaches 86.03% and the purity is 97.42%.

参考文献/References:

［1］史法胜.N苯基马来酰亚胺的合成研究［J］.山东化工,2008,37:1620.
［2］崔健.N苯基马来酰亚胺的合成研究进展及应用［J］.现代塑料加工应用,2001,13(2):5355.
［3］贾海红,郑纯智,刘玮炜.N苯基马来酰亚胺的合成及应用进展［J］.热固性树脂,2004,19(1):3638,44.
［4］王新江,还兰红.N苯基马来酰亚胺的应用与合成［J］.化学工业与工程技术,2001,21(1):1926.
［5］张建华.N苯基马来酰亚胺的应用及合成技术进展［J］.河南化工,2002(9):67.
［6］李海燕,潘锦.ABS树脂耐热改性剂N苯基马来酰亚胺［J］.精细与专用化学品,2001,10(10):2526,28.
［7］梁西良,薛用强,郑雪岩,等.N苯基马来酰亚胺合成方法［J］.化学与粘合,2000,22(2):8586.
［8］贾海红,郑纯智,刘玮炜.N苯基马来酰亚胺的合成及应用进展［J］.热固性树脂,2004.19(1):36,38.
［9］Tsumura,Ryuichiro.Preparation process of Nsubstitued maleimides［P］.EP 0403240,19901219.
［10］GALINSKI M,LEWANDOWSKI A,STEPNIAK I.Ionic liquids as electrolytes［J］.Electrochimica Acta,2006,51:5567.

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