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[1]李晶,杨效军,徐旺生*.溶胶凝胶法制备纳米钛酸铅的工艺[J].武汉工程大学学报,2010,(11):15-17.[doi:10.3969/j.issn.16742869.2010.11.004]
　LI Jing,YANG Xiao jun,XU Wang sheng.Research on preparation process of nanolead titanate by solgel method[J].Journal of Wuhan Institute of Technology,2010,(11):15-17.[doi:10.3969/j.issn.16742869.2010.11.004]
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《武汉工程大学学报》[ISSN:1674-2869/CN:42-1779/TQ]

卷:
期数:
2010年11期
页码:
15-17
栏目:
化学与化学工程
出版日期:
2010-11-30

文章信息/Info

Title:
Research on preparation process of nanolead
titanate by solgel method
文章编号:
16742869(2010)11001503
作者:
李晶; 杨效军; 徐旺生*
武汉工程大学化工与制药学院,绿色化工过程省部共建教育部重点实验室,湖北 武汉 430074
Author(s):
LI Jing;  YANG Xiaojun;  XU Wangsheng
School of Chemical Engineering & Pharmacy, Wuhan Institute of Technology, Key Laboratory for
Green Chemical Process of Ministry of Education, Wuhan 430074, China
关键词:
溶胶凝胶法; 纳米; 钛酸铅
Keywords:
solgel method; nano; lead titanate
分类号:
TB383
DOI:
10.3969/j.issn.16742869.2010.11.004
文献标志码:
A
摘要:
采用无机溶胶凝胶的方法来制备纳米钛酸铅粉体,以廉价的无机钛盐为原料,有效克服了传统方法因采用有机钛盐或有机钛而导致的生产成本过高的缺点,并利用XRD、FTIR、SEM等分析手段对样品的颗粒大小、结构和形貌进行了表征.研究结果表明：制备出的PbTiO3干凝胶在1 000 ℃下热处理2 h可以得到结晶程度很好的纳米PbTiO3粉体.
Abstract:
The powder of nanolead titanate is produced by inorganic solgel method. In this new route, the inexpensive inorganic titanium salt is a raw material, which effectively overcomes the shortcomings of high costs caused by the use of organic Lead salt or organic titanium, and the structure and particle size and morphology of nanometer PbTiO3 powder were characterized by XRD, FTIR, SEM. The results show that the dried PbTiO3 gel is highly crystallized after heat treatment at 1 000 ℃ for 2 h.

参考文献/References:

［1］张素芳,翟学良.钛酸铅系电子陶瓷及粉体的制备方法［J］.无机盐工业,2003,35(3):1316.
［2］ZENG X H,LIU Y Y,WANG X Y,et a1.Preparation of nanoerystalline PbTiO3 by accelerated solgel process［J］.Mater Chem Phys,2003,77:209214.
［3］Blum J B,Garkovich S R.Solgel derived PbTiO3［J］.Journal of Materials Science,1985(20):44794483.
［4］田红梅,毕宇,徐旺生.溶胶凝胶法制备纳米钛酸钡［J］.武汉工程大学学报,2010,32(3):2830.
［5］孙宇澄,石维.钛酸铅压电陶瓷的制备及应用［J］.电子元件与材料,2009,28(9):3437.
［6］胡亚伟,田克情.溶胶凝胶法制备钛酸铅陶瓷纤维热处理条件的研究［J］.河北省科学院学报,2009,26(2)：4953.
［7］顾期斌,刘云才. PbTiO3纳米材料制备方法［J］.湖北第二师范学院学报,2008,25(8):3941.
［8］张昭,彭少方,刘栋昌,等.无机精细化工工艺学［M］.北京:化学工业出版社,2005:5368.
［9］孙召明,姜峰.电子陶瓷材料—钛酸铅的制备与应用［J］.湖南有色金属,2000,16(6)：2427.
［10］Kuo Y F, Tseng T Y.Preparation and characterization of PLZT thin fims by solgel processing ［J］.J of Mater Sci,1996,31:63616368.

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备注/Memo

备注/Memo:
张瑞收稿日期:20100705作者简介:李晶(1984),女,湖北随州人,硕士研究生.研究方向:无机精细化工.指导老师:徐旺生,教授,硕士研究生导师.研究方向:化学工艺
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