|本期目录/Table of Contents|

[1]陈求索,余海湖*,黄金山,等.钒氧化物纳米管的制备与表征[J].武汉工程大学学报,2009,(05):54-56.
 CHEN Qiu suo,YU Hai hu,HUANG Jin shan,et al.Preparation and characterization of vanadium oxide nanotubes[J].Journal of Wuhan Institute of Technology,2009,(05):54-56.
点击复制

钒氧化物纳米管的制备与表征(/HTML)
分享到:

《武汉工程大学学报》[ISSN:1674-2869/CN:42-1779/TQ]

卷:
期数:
2009年05期
页码:
54-56
栏目:
化学与化学工程
出版日期:
2009-05-28

文章信息/Info

Title:
Preparation and characterization of vanadium oxide nanotubes
文章编号:
16742869(2009)05005403
作者:
陈求索1余海湖12*黄金山1吴银伟1史勇1
1.武汉理工大学光纤传感技术与信息处理教育部重点实验室;
2.材料复合新技术国家重点实验室,武汉 430070
Author(s):
CHEN Qiusuo1YU Haihu12HUANG Jinshan1WU Yinwei1SHI Yong1
1.Key Lab of Fiber Optic Sensing Technology and Information Processing of Ministry of Education;
2.State Key Lab ofAdvanced Technology for Materials Synthesis and Processing,Wuhan University of Technology,Wuhan 430070,China
关键词:
钒氧化物纳米管水热法
Keywords:
Vanadium oxidenanotubehydrothermal method
分类号:
O611.4;O614.51+1
DOI:
-
文献标志码:
A
摘要:
以V2O5粉末、十六胺为主要原料,采用水热法制得钒氧化物纳米管,采用SEM、TEM、XRD、FTIR对纳米管进行了表征.生成的纳米管长度约为1~5 μm,直径约为30~80 nm.在水热反应条件下,十六胺与钒酸盐前驱体发生插层反应,形成板层结构,板层结构表面的几层脱离母体,形成钒氧化物-有机物薄层,薄层发生卷曲,逐步形成钒氧化物纳米管.
Abstract:
V2O5 powder and hexadecylamine were used as main raw materials,and vanadium oxide nanotubes were prepared through the hydrothermal method.The nanotubes were characterized with SEM,TEM,XRD and FTIR.The obtained nanotubes are with length of 1~5 μm and diameter of 30~80 nm.The formation mechanism of the nanotubes is as follow: lamellar structures form as the intercalation takes place between hexadecylamine and vanadate precursor under the hydrothermal environment.Some top layers on the parent materials peel off and scroll into tubes gradually with the curl of their edges.

参考文献/References:

[1]Xia Y N,Yang P D,Sun Y G,et al.Onedimensional nanostructures: synthesis,characterization,and applications [J].Ad Mater,2003,15(4):353-389.
[2]GomezNavarro C,P J de Pablo,Colchero J,et al.Probing electrical transport in nanowires: current maps of individual V2O5 nanofibres with scanning force microscopy [J].Nanotechnology,2003,14: 134-137.
[3]Pang S P,Li G C,Zhang Z K,et al.Synthesis of polyanilinevanadium oxide nanocomposite nanosheets [J].Rapid Commun,2005,26: 1262-1265.
[4]Li G C,Pang S P,Jiang L,et al.Environmentally friendly chemical route to vanadium oxide singlecrystalline nanobelts as a cathode material for lithiumion batteries [J].J Phys Chem B,2006,110: 9383-9386.
[5]Liu J,Wang X,Peng Q,et al.Vanadium pentoxide nanobelts: highly selective and stable ethanol sensor materials [J].Adv Mater,2005,17(6): 764-767.
[6]Gu G,Schmid G,Chiu P W,et al.V2O5 nanofibre sheet actuators [J].Nature Materials,2003,(2):316-319.
[7]陈文,彭俊锋,麦立强,等.两种一维纳米结构钒氧化物的合成与表征 [J].无机化学学报,2004,20(2):147-151.
[8]Doubley A.Synthesis and characterization of novel oxide compounds using surfactant templates.[D].Binghamton:State University of New York,2001.
[9]Dwyer C O,Navas D,Lavayen V,et al.Nanourchin: the formation and structure of highdensity spherical clusters of vanadium oxide nanotubes [J].Chem Mater,2006,18: 3016-3022.
[10]Chen X,Sun X,Li Y.Selfassembling vanadium oxide nanotubes by organic molecular templates [J].Inorg Chem,2002,41(17): 4524-4530.

相似文献/References:

备注/Memo

备注/Memo:

收稿日期:20090107
基金项目:国家自然科学基金重点项目(No.60537050)
作者简介:陈求索(1985),男,湖南湘潭人,硕士研究生.研究方向:光电子与信息材料.
指导老师:余海湖,男,博士,教授,博士生导师.研究方向:光电子与信息材料. *通信联系人.
更新日期/Last Update: