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[1]姜铁坤,吴江渝,肖夏,等.微波条件下树形分子核单元的合成及优化[J].武汉工程大学学报,2010,(11):70-72.[doi:10.3969/j.issn.16742869.2010.11.018]
　JIANG Tie kun,WU Jiang yu,XIAO Xia,et al.Microwave assisted synthesis of core unit of PAMAM dendrimer[J].Journal of Wuhan Institute of Technology,2010,(11):70-72.[doi:10.3969/j.issn.16742869.2010.11.018]
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微波条件下树形分子核单元的合成及优化(/HTML)
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《武汉工程大学学报》[ISSN:1674-2869/CN:42-1779/TQ]

卷:
期数:
2010年11期
页码:
70-72
栏目:
资源与土木工程
出版日期:
2010-11-30

文章信息/Info

Title:
Microwave assisted synthesis of core unit of PAMAM dendrimer
文章编号:
16742869(2010)11007003
作者:
姜铁坤; 吴江渝; 肖夏; 林希; 郭三维
武汉工程大学材料科学与工程学院,湖北 武汉 430074
Author(s):
JIANG Tiekun;  WU Jiangyu;  XIAO Xia;  LIN Xi;  GUO Sanwei
School of Material Science and Engineering,Wuhan Institute of Technology,Wuhan 430074,China
关键词:
微波辅助合成; 聚酰胺胺; 树形分子; 核单元
Keywords:
microwave assisted synthesis;  polyamidoamine;  dendrimers;  core unit
分类号:
O633.4
DOI:
10.3969/j.issn.16742869.2010.11.018
文献标志码:
A
摘要:
聚酰胺胺树形分子因其独特的分子结构使其在药物载体、生物化学、催化剂等方向有着潜在的应用.但常温下合成树形分子的周期较长,致使其成本高.从乙二胺出发,利用微波技术,通过反复摸索,优化得到了微波辅助合成聚酰胺胺树形分子核单元的最佳条件.
Abstract:
Polyamidoamin(PAMAM) dendrimers have received extensive attentions in biological and chemical fields due to their unique molecular strures. However, the traditional method to obtain PAMAM dendrimer is a rough and timeconsuming process, resulting in a high synthesis cost.At this point, we employed microwave assisted process to synthesize PAMAM dendrimer core from ethylenediamine, and the optimization of the reaction conditions was investigated.

参考文献/References:

［1］Prabal K Maiti, Tahir Cagin, Guofeng Wang,et al. Goddard structure of PAMAM dendrimers: generation 1 through 11［J］.Macromolecules,2004,37:62366254.
［2］Ronald C Hedden, Barry J Bauer, A Paul Smith,et al.Templating of inorbanic nanoparticles by PAMAM/PEG dendrimerstar polymers［J］.Polymer,2002,43:54735481.
［3］Abhay S Chauhan, S Sridevi, Kishore B Chalasani,et al.Dendrimermediated transdermal delivery:enhanced bioavailability of indomethacin［J］.Journal of Controlled Release,2003,90:335343.
［4］Pelle Lidstrom, Jason Tierney, Bernard Wathey,et al.Microwave assisted organic synthesis a review［J］.Tetrahedron,2001,57:92259283.
［5］Gedye R N,Wei J B.Rate enhancement of organic reactions by microwaves at atmospheric pressure［J］.Can J Chem,1998,76:525532.
［6］Bosman A W,Janssem H M,Meiler E W.About dendrimers: structure, physical properties and applications, Chem. Rev,1999,99:16651688.
［7］J Peterson a, V Allikmaa, J Subbi,et al.Structure deviations in poly(amidoamine) dendrimers: a MALDITOF MS analysis［J］.Eur:Polym J,2003,39:3342.

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备注/Memo

备注/Memo:
龚晓宁收稿日期:20100709基金项目:武汉市青年科技晨光计划项目(200950431195)作者简介:姜铁坤(1986),男,湖北鄂州人,硕士研究生.研究方向:材料加工工程.指导老师:吴江渝,博士,硕士生导师.研究方向:生物医用高分子.
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