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[1]戴丽雯,陈文利,巨修练*.环氧啉含量的HPLC法测定方法[J].武汉工程大学学报,2011,(12):27-29.
　DAI Li wen,CHEN Wen li,JU Xiu lian.Determination of cycloxylidin by HPLC[J].Journal of Wuhan Institute of Technology,2011,(12):27-29.
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《武汉工程大学学报》[ISSN:1674-2869/CN:42-1779/TQ]

卷:
期数:
2011年12期
页码:
27-29
栏目:
化学与化学工程
出版日期:
2011-12-30

文章信息/Info

Title:
Determination of cycloxylidin by HPLC
文章编号:
16742869(2011)12002703
作者:
戴丽雯1; 陈文利2; 巨修练1*
1.武汉工程大学化工与制药学院，湖北省新型反应器与绿色化学工艺重点实验室,湖北 武汉 430074；
2.武汉工程大学分析测试中心，湖北 武汉 430074
Author(s):
DAI Liwen1; CHEN Wenli2; JU Xiulian1
1.School of Chemical Engineering ＆ Pharmacy,Hubei Key Laboratory of Novel Reactor and Green Chemical Technology,
Wuhan Institute of Technology,Wuhan 430074,China；
2.Center of Analysis and Test,Wuhan Institute of Technology,Wuhan 430074,China
关键词:
环氧啉; 高效液相色谱法; 质量控制
Keywords:
cycloxylidin; HPLC; quality control
分类号:
R927.2
DOI:
-
文献标志码:
AAdoi:10.3969/j.issn.16742869.2011.12.006
摘要:
建立了环氧啉的高效液相色谱（HPLC）的测定方法，在C18色谱柱（C18250 mm×4.6 mm,5 μg/mL）上，以甲醇水（2575,V/V）为流动相，在流速为1.0 mL/min，室温条件下，220 nm波长检测，环氧啉标准样品分离效果良好.环氧啉溶液在43.2~345.6 μg/mL范围内浓度与峰面积线性关系良好，相关系数r=0.999 92；方法的检测限为0.4 μg.该方法简单快速，准确，可靠，为环氧啉的工业生产质量控制提供一定的保证.
Abstract:
The method for the determination of Cycloxylidin by high performance liquid chromatography (HPLC) was established.It used C18 column (250 mm×4.6 mm, 5 μg/mL) to separate the sample,25% methanol and 75% water as the mobile phase,and the Cycloxylidin was detected at 220 nm with the flow rate of 1.0 mL/min at ambient temperature.The result showed that the linear relative coefficient was 0.999 92 while in a range of 43.2—345.6 μg/mL;the limit of this method was 0.4 μg.This method was simple,rapid and effective in the quality control for production of Cycloxylidin.

参考文献/References:

［1］李黎,巨修练.绿色农药环氧啉的开发及应用［J］.湖北植保,2009,115（5）：556.
［2］杨吉春,李淼,柴宝山,等.新烟碱类杀虫剂最新研究进展［J］.农药,2007,46（7）：433438.
［3］史晓斌,王鹏.吡虫啉的抗性现状及其机理研究进展［J］.农药研究与应用,2010,14（2）:13.
［4］周琴,吴永凤.吡虫啉的高效液相色谱法分析［J］.广东化工,2004,31（1）:2829.
［5］巨修练,卢伦,李黎.1(1,2环氧丙基)N硝基亚咪唑烷2基胺的制备及用途：中国，200810236885.X［P］.20090812.

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